FREE COLE-PARMER CATALOG ON CD

February 26, 2010

2009/10 Cole-Parmer®<br>General Catalog2009/10 Cole-Parmer® General Catalog — Digital Edition

Find everything you need inside our NEW General Catalog! This 2,600-page catalog features over 60,000 products for electrochemistry, fluid handling, industrial process, laboratory research, and more. See our vast selection of hard-to-find items and everyday basics—including over 10,000 new products—from the industry’s most respected brands. 

This user-friendly CD contains everything in our printed Cole-Parmer General Catalog, plus links to our Web site for the most current product information, pricing, and availability.

Get mine today!

 2009/10 Cole-Parmer General Catalog, Digital Edition


FREE 2600 PAGE COLE-PARMER CATALOG!

February 24, 2010

2009/10 Cole-Parmer®<br>General Catalog2009/10 Cole-Parmer® General Catalog—Find everything you need inside our NEW General Catalog! This 2,600-page catalog features over 60,000 products for electrochemistry, fluid handling, industrial process, laboratory research, and more. See our vast selection of hard-to-find items and everyday basics—including over 10,000 new products—from the industry’s most respected brands.  Get mine today!


Hey Smarty Pants, Take our Tech Challenge on Circuit Board Failures.

February 22, 2010

Tech Challenge 

 

 

Challenge: A manufacturer of electrical test equipment noticed that circuit board failures increased during the fall and winter, and decreased during the spring and summer months. After a thorough investigation of the failures, it was determined that certain individual components on the circuit boards were damaged internally.

Which of the following actions should be taken:

  1. Install a cleanroom and implement cleanroom procedures
  2. Increase the number of inspections of individual components before installing them on the circuit boards.
  3. Rotate component stock to see if older stock is the source of the failures.
  4. Add a surge protector, as quite often a power surge will damage the circuit board.
  5. Implement a static control program.

See the answer.


Temperature Calibration in Industrial Processes. Woo-hoo!

February 19, 2010

 

Temperature is one of the most frequently measured parameters in industrial processes. A wide variety of mechanical and electrical thermometers are used to sense and control process temperatures. Regular calibration of these thermometers is critical to ensuring consistent quality of product manufactured, as well as providing regulatory compliance for some industries.

 

The Basics

Most simply stated, temperature calibration consists of placing a thermometer under test into a known, stable temperature environment. A comparison is made between the actual temperature and the reading indicated by the thermometer under test and the difference is noted.

Adjustments can then be made either directly to the thermometer or to its readout. Electrical thermometers are adjusted by mathematically re-creating the coefficients used by SMART transmitters or other readout devices to translate their electrical output to temperature. Many mechanical thermometers, such as dial gauges can be adjusted by turning a dial or other mechanical device. In some cases, such as liquid-in-glass thermometers, direct adjustments are not possible and offsets must be noted.

In industrial applications, the temperature environment is usually provided by a drywell, or “dry-block” calibrator, or a micro-bath. Both offer portability and a wide range of temperatures. Drywells use high stability metal blocks with drilled wells to accept the reference and UUT. Drywells typically cover ranges from -45°C to 1200°C and micro-baths cover ranges from -25°C to 200°C. Micro-baths are similar in size to drywells but use a small tank of stirred fluid instead of a metal block. Micro-baths offer significant advantages when calibrating short or odd shaped probes.

The “actual” temperature of the bath or dry-well is determined by a reference thermometer, which may be either a thermometer internal to the heat source or an external reference thermometer operating independent of the heat source.

Figure 1: Heat source as reference standard

External or Internal Reference

Micro-baths and dry-wells have a built-in sensor to provide a feedback loop to the unit’s controller and to provide a temperature reading to the user. The manufacturer of the heat source (or a third-party laboratory) can calibrate this sensor so the unit displays a traceable temperature within a stated uncertainty. For some applications, this uncertainty level (typically ±1-2°F) is adequate. Using an internal reference is sometimes preferred because it requires fewer instruments and enhances portability for field applications. This method is illustrated in Figure 1.

The reference system, however, should be more accurate than the process system being calibrated. The generally accepted Test Uncertainty Ratio (TUR) is 4:1 (i.e. the reference should be four times more accurate than the sensor or system being calibrated). Therefore, if a process thermometer is being relied on for correct readings within ±2°F, the test system should typically be ±0.5°F or better at each temperature in question. As a general rule, temperature uncertainties are larger at higher temperatures.

Figure 2: External reference standard

Where uncertainty requirements are more rigorous, external reference thermometers help improve system uncertainty (see Figure 2). These thermometers—usually platinum resistance thermometers (PRTs) or thermistors—can often be calibrated to a few hundredths of a degree and can be read by electronic readout devices that contribute little to total measurement uncertainty. These systems can provide measurements with uncertainties as low as ±0.05°F or ±0.02°F—or better. The reference probe and readout should be periodically re-calibrated, preferably by an accredited cal lab, to assure performance specifications and maintain traceability.

Because external thermometers are more accurate, they increase the relative significance of other components of calibrations uncertainty, such as uniformity and stability. It is, of course, critical in any calibration to account for all sources of uncertainty in the process.

System or Component Calibrations

Most temperature sensors used in processes are read by transmitters, which send a 4 to 20 mA signal to a control panel, which then displays the temperature for process monitoring. Such systems involve three instruments, all of which require periodic calibration. Of these three, the largest errors are often found in the temperature sensor (which is subject to drift for a variety of reasons), so its calibration is of particular concern.

More Details
or Order Online:

Hart Scientific Field Temperature Dry Wells

High-Temperature Field Dry Block Calibrator

Industrial Dual-Block Calibrator

Several calibration methodologies are used in the process plant with the most representative method being to calibrate the complete measurement system from sensor through transmitter to indicator or controller; alternatively each component of the measurement system can be individually calibrated.

The temperature sensor can be individually calibrated using a drywell or micro-bath heat source to simulate the process temperature. If the temperature sensor is electrical, a readout device measures its output. Adjustments are then made to the thermometer or its coefficients as discussed earlier.

The transmitter is calibrated using a precision simulator to generate the resistance or voltage output from the temperature sensor and input to the transmitter. The simulator also measures the resulting transmitter current or voltage output. The transmitter is adjusted to ensure that the output follows the input, e.g. for a 4 to 20 mA transmitter with a range of 0°C to 200°C, 4 mA corresponds to 0°C and 20 mA corresponds to 200°C. The simulator provides a wide range of input and output ranges to cover all resistance thermometer and thermocouple types.

The indicator or controller is also calibrated using a precision simulator to generate simulate the resistance or current input from the transmitter. The indicator or controller is adjusted so that the display variable matches the simulated input.

The complete system is calibrated using the drywell or micro-bath to compare the reference probe and UUT. The transmitter is adjusted to ensure that the indicator or controller agrees with the reference probe readout. This calibration method is most representative of the real process, is faster and simpler to perform.

Accredited Calibration Services

Calibration of the thermometer standards used to calibrate industrial thermometers provides traceability, which means that measurements are traceable to national and international standards. Traceability to international standards ensures that measurements made in one country agree with measurements in another country, which is particularly important for companies using similar manufacturing processes at different locations around the world.

More Details
or Order Online:

InnoCal Calibration Services

More and more calibration labs throughout the U.S. are being accredited to international standards such as the ISO Guide 25. Accreditation ensures that a lab’s quality systems, uncertainty levels, and traceability statements have been examined and independently verified. NVLAP and A2LA are the primary accrediting bodies in the U.S. A recently signed international agreement ensures that accrediting bodies in almost every developed nation also recognize accreditations granted by NVLAP and A2LA.

In summary, process plant temperature calibrations require a good reference thermometer with readout, a drywell and/or micro-bath heat source, and a precision simulator. These instruments, in turn, should be periodically calibrated by a reputable lab, preferably one that is accredited and can prove traceability.

How to Determine Thermocouple System Accuracy
Temperature Controller Features
Temperature Conversion Equations
Temperature Instrument Ranges

View original article.

by Bernard Morris, Vice-President of Sales, Hart Scientific, Inc.
Reprinted with permission of Hart Scientific, Inc.


Want to measure some voltage? Read our intro on Oscilloscopes.

February 17, 2010

This introduction to digital storage oscilloscopes (DSOs)
takes you on a quick but comprehensive tour of DSO
functions and measurements.

An oscilloscope measures and displays voltage signals on a time-versus-voltage graph. In most applications the graph shows how the signal changes over time: the vertical (Y) axis represents voltage, and the horizontal (X) axis represents time. This simple graph can tell you many things about a signal:

    • View the signal for glitches.
    • Calculate the frequency of an oscillating signal.
    • Tell if a malfunctioning component is distorting the signal.
    • Tell how much of the signal is noise and whether the noise is changing with time.

Today’s handheld digital storage oscilloscopes offer two critical advantages over benchtop models: they are battery-operated, and they use isolated, electrically floating inputs. These designs make safety-certified measurements possible in 1000V CAT II and 600V CAT III environments — a critical need for safely troubleshooting electrical devices in high-energy applications.

Scopemeters Far left: The Fluke 190 Series ScopeMeter has a 200 MHz bandwidth and 2.5 GS/s real-time sampling rate.

Left: The Fluke 123 ScopeMeter with 20 MHz dual-input measurement shows both meter reading and waveform.

Time/Volt/Graph Figure 1. Time-versus-voltage graph.

Scopes and DMMs
The difference between an oscilloscope and a DMM (digital multimeter) can be summarily stated as “pictures vs. numbers.” A DMM is a tool for making precise measurements of discrete signals, enabling readings of up to eight digits of resolution for the voltage, current or frequency of a signal. On the other hand, it cannot depict waveforms visually to reveal signal strength, waveshape, or the instantaneous value of the signal. Nor is it equipped to reveal a transient or a harmonic signal that could compromise the operation of a system.

A scope adds a wealth of information to the numeric readings of a DMM. While displaying instantaneous numerical values of a wave, it also reveals the shape of the wave, including its amplitude (voltage) and frequency. With such visual information, a transient signal that may pose major consequences to a system can be displayed, measured and isolated.

Reach for a scope if you want to make both quantitative and qualitative measurements. Use a DMM to make high-precision checks of voltage, current, resistance and other electrical parameters.

Sampling
Sampling is the process of converting a portion of an input signal into a number of discrete electrical values for the purpose of storage, processing and display. The magnitude of each sampled point is equal to the amplitude of the input signal at the time the signal is sampled. The input waveform appears as a series of dots on the display. If the dots are widely spaced and difficult to interpret as a waveform, they can be connected using a process called interpolation, which connects the dots with lines, or vectors.

Triggering
Trigger controls allow you to stabilize and display a repetitive waveform.

Edge triggering is the most common form of triggering. In this mode, the trigger level and slope controls provide the basic trigger point definition. The slope control determines whether the trigger point is on the rising or the falling edge of a signal, and the level control determines where on the edge the trigger point occurs.

For even greater control and visibility into signal phenomena, you can use the ability of some DSOs to capture events leading up to the trigger point (“pre-trigger”) or after the trigger point (“posttrigger”) on the input waveform. As one example, by using pretriggering or post-triggering, you may catch a spike that occurs in between two occurrences of a signal.

Pulse width triggering triggers on specific pulses within a series or it can identify one-time or sporadic problems in a pulsed signal. In this mode, you can monitor a signal indefinitely and trigger on the first occurrence of a pulse whose duration, or pulse width, is either outside of or within set limits. The goal is to isolate and display a pulse that meets the predetermined time criteria.

Single-shot triggering is useful for capturing a one-time event — such as electrical arcing or a relay closure. A DSO with a single-shot mode waits until it receives a trigger and then sets itself in a hold mode to store the signal at the moment the onetime event occurs.

Video triggering is a powerful feature of advanced DSOs. Video signals can be extremely complex, providing no unique edge that is repetitive and that can be isolated to stabilize the signal. With an extensive range of signaling protocols in use in today’s electronicvideo equipment and systems, an effective DSO is one that recognizes the predominant video protocols and provides appropriate triggering functionality.

Sampling Graph Figure 2. Sampling and interpolation.

Setup The task of capturing and analyzing an unknown waveform on an oscilloscope can be routine, or it can seem like taking a shot in the dark. However, in most cases, taking a methodical approach to setting the oscilloscope will capture a stable waveform or help you determine how the scope controls need to be set so that you can capture the waveform.

1) Start with Auto Connect the ground reference lead and then connect the probe tip to the circuit test point. Most oscilloscopes have the ability to either perform a one-time auto setup or continuously analyze the unknown input signal. Press the AUTO button or verify that the scope is already in Auto mode.

Pressing the AUTO button will typically set up the oscilloscope to automatically adjust three key parameters:

Vertical sensitivity. Adjusts the vertical sensitivity so that the vertical amplitude spans approximately three to six divisions.

3-6 Vert Graph Figure 3. Unknown trace adjusted for 3-6 vertical divisions.

Horizontal timing. Adjusts the horizontal time per division so that there are three to four periods of the waveform across the width of the display.

3-4 Horizontal Graph Figure 4. Unknown trace adjusted for 3-4 periods horizontally.

Trigger position. Sets the trigger position to the 50 % point of the vertical amplitude. Depending on the signal characteristics, this action may or may not result in a stable display.

Trigger Point Figure 5a. Trigger point set to 50% point on trace.

Trigger Second Period Figure 5b. Trigger point is set to the 50 % point but due to the aberration on the leading edge in the second period, an additional trigger results in an unstable display.

At this point you should see a trace that 1) lies within the vertical range of the display, 2) shows at least three periods of a waveform, and 3) is stable enough to allow you to recognize the overall characteristics of the waveform. Next, start fine-tuning the settings.

2) Adjust vertical and horizontal settings Start by adjusting the horizontal timing, increasing the time per division so that you see a wide time span of the unknown waveform. From that view, reverse the adjustment as required to narrow the view to just what you want to display.

Now adjust the vertical sensitivity, expanding the waveform vertically but ensuring that the high and low points of the waveform do not exceed the vertical span.

3) Adjust trigger settings If needed, adjust the trigger settings to stabilize the waveform display. Or, you may want to adjust the trigger delay to see pre- or post-trigger details on the waveform. Always start with the trigger-level setting, adjusting it so that it falls on a repetitive, unique point on the rising or falling edge of a waveform.

As an example, with the oscilloscope trigger set to the rising edge and the level set to the 50 % point, the following figures illustrate the cause of an unstable waveform display.

First Trig Point Figure 6a. At the first update, the scope triggers on the first edge. On the second update, the scope may trigger on the second trigger point indicated.

After two successive updates based on triggers 1 and 2, the resultant trace will appear unstable.

Unstable Wave Figure 6b. Unstable waveform display caused by incorrect trigger level setting.

However, simply by manually adjusting the trigger point to a repetitive, unique point on the edge, you can solve this problem and produce a stable waveform display.

Repetitive Graph Figure 6c. Trigger level adjusted to a unique repetitive position, outside the aberration on the second period.

When working with complex signals like a series of pulses, pulse width triggering may be required. With this technique, both the trigger-level setting and the next falling edge of the signal must occur within a specified time span. Once these two conditions are met, the oscilloscope triggers.

Specific Pulse Figure 7. Pulse width triggering will allow you to set up the oscilloscope to trigger on a specific pulse defined by level and time.

Another technique is singleshot triggering, by which the oscilloscope will display a trace only when the input signal meets the set trigger conditions. Once the trigger conditions are met, the oscilloscope acquires and updates the display, and then freezes the display to hold the trace.

Understanding and reading waveforms
The majority of electronic waveforms encountered are periodic and repetitive, and they conform to a known shape. Here are the factors to consider in analyzing waveforms:

Shape. Repetitive waveforms should be symmetrical. That is, if you were to print the traces and cut them in two like-sized pieces, the two sides should be identical. A point of difference could indicate a problem.

Non Symmetrical Grph Figure 8. If the two components of the waveform are not symmetrical, there may be a problem with the signal.

Rising and falling edges. Particularly with square waves and pulses, the rising or falling edges of the waveform can greatly affect the timing in digital circuits. It may be necessary to decrease the time per division to see the edge with greater resolution.

Cursors/Graticule Figure 9. Use cursors and the graticule marks to evaluate the rise and fall times of the leading and trailing edges of a waveform.

Amplitude. Verify that the level is within the operating specifications of the circuit. Also check for consistency, from one period to the next. Monitor the waveform for an extended period of time, watching for any changes in amplitude.

Horizontal Cursors Figure 10. Use horizontal cursors to identify amplitude fluctuations.

Amplitude offsets. DC-couple the input and determine where the ground reference marker is. Evaluate any DC offset and observe if this offset remains stable or fluctuates.

DC Offsets Figure 11. Evaluate waveform DC offsets.

Periodic waveshape. Oscillators and other circuits will produce waveforms with constant repeating periods. Evaluate each period in time using cursors to spot inconsistencies.

Period/Period Figure 12. Evaluate period-to-period time changes.

Waveform anomalies Here are typical anomalies that may appear on a waveform, along with the typical sources of such anomalies.

Transients or glitches. When waveforms are derived from active devices such as transistors or switches, transients or other anomalies can result from timing errors, propagation delays, bad contacts or other phenomena.

Transient Figure 13. A transient is occurring on the rising edge of a pulse.

Noise. Noise can be caused by faulty power supply circuits, circuit overdrive, crosstalk, or interference from adjacent cables. Or, noise can be induced externally from sources such as DC-DC converters, lighting systems and high-energy electrical circuits.

Ground Reference Figure 14. A ground reference-point measurement showing induced random noise.

Ringing.
Ringing can be seen mostly in digital circuits and in radar and pulse-width-modulation applications. Ringing shows up at the transition from a rising or falling edge to a flat DC level. Check for excessive ringing, adjusting the time base to give a clear depiction of the transitioning wave or pulse.

Excessive Ringing Figure 15. Excessive ringing occurring on the top of the square wave.

Momentary fluctuation. Momentary changes in the measured signal generally result from an external influence such as a sag or surge in the mains voltage, activation of a high-power device that is connected to the same electrical grid, or a loose connection. Use the DSO’s slowest timebase setting or the paperless recording or “roll” mode. Start at the input and watch the acquired waveform over long time spans to track down the source of the problem.

Momentary Change Figure 16a. A momentary change of approximately
1.5 cycles in the amplitude of the sinewave.
Plotting Amplitude Figure 16b. Using an oscilloscope with a paperless recorder mode allows plotting of the amplitude (voltage level) over time.

Drift. Drift — or minute changes in a signal’s voltage over time — can be tedious to diagnose. Often the change is so slow that it is difficult to detect. Temperature changes and aging can affect passive electronic components such as resistors, capacitors and crystal oscillators. One problematical fault to diagnose is drift in a reference DC voltage supply or oscillator circuit. Often the only solution is to monitor the measured value (V dc, Hz, etc.) over an extended time.

Freq. Measurement Figure 17. Performing a frequency measurement on a crystal oscillator that has been trend-plotted over an extended period (days or even weeks) can highlight the affect of drift caused by temperature changes and aging.

Diagnosing problems Although successful troubleshooting is both an art and a science, adopting a troubleshooting methodology and relying on the functionality of an advanced DSO can greatly simplify the process.

Good troubleshooting practices will save time and frustration. The time-tested approach known as KGU, Known Good Unit comparison, accomplishes both goals. KGU builds on a simple principle: an electronic system that is working properly exhibits predictable waveforms at critical nodes within its circuitry, and these waveforms can be captured and stored. This reference library can be stored right on the DSO as an online resource, or can be printed out to serve as a hardcopy reference document. If the system or an identical system later exhibits a fault or failure, waveforms can be captured from the faulty system — called the device under test (DUT) — and compared with their counterparts in the KGU. Consequently, the DUT can either be repaired or replaced.

To build a reference library, start by identifying appropriate test points, or nodes, on the DUT. Now, run the KGU through its paces, capturing the waveform from each node. Annotate each waveform as required.

Get into the habit of always documenting key waveforms and measurements. Having a reference to compare to will prove invaluable during future troubleshooting

Troubleshooting
Whichever troubleshooting scenario below is appropriate at the time, remember that it’s important to inspect waveforms for fast-moving transients or glitches, even if a spot check of the waveform reveals no anomalies. These events can be difficult to spot, but the high sampling rate of today’s DSOs, together with effective triggering, makes it possible.

DUT with KGU. This approach assumes that you have access to a KGU and a reference library.

    1. Make sure the DUT and KGU are set up in identical operating modes.
    2. Starting at a high-level point in the system or block diagram, use the DSO to look for the presence or absence of fundamental signals. For example, look for a line-voltage supply, as well as subsequent DC supply voltages to the various subsystems. This requires probing the major input and output signals at major nodes in the system.
    3. Compare signals at key nodes while changing the operating mode to see if a failure occurs. With signals from both devices available, you have two options:

• Display the live waveform from the KGU on Channel 1 of the DSO, and display the live waveform from the DUT on Channel 2.

• Capture a trace from the KGU and overlay it with a trace from the DUT. Perform a waveform-compare or pass/fail test.

    4. Continue with this process until you note a variance between the DUT and KGU waveforms.

DUT with Circuit Diagrams. This approach assumes that no KGU and no waveform reference library for the DUT are available, but that circuit diagrams of the DUT can be located.

    1. Review the circuit diagrams to understand the basic operation of the DUT.

• Analog circuits such as oscillators, amplifiers and signal conditioners (attenuators, filters and dividers) should exhibit uniform waveform patterns.

• Digital circuits such as gates, switches and processors should display waveforms with predictable amplitudes, pulse periods and even pulse patterns.

    2. Starting at a high-level point in the system or block diagram, use the DSO to look for the presence or absence of fundamental signals. For example, look for a line-voltage supply, as well as subsequent DC supply voltages to the various subsystems. This requires probing the major input and output signals at major nodes in the system.
    3. Use the storage capability of the DSO to capture and compare waveforms while changing the operating mode of the DUT.

• Visualize a theoretical “good” waveform and compare it to the waveform displayed on the DSO. Try to identify any obvious anomalies.

 

    4. Use the horizontal or vertical cursors to quickly evaluate if the time or amplitude of the trace falls within the time or amplitude ranges suggested by the circuit design.

Complex DUT, No Circuit Diagrams. This approach assumes that the DUT is a fairly complex system, that no KGU is available, and that only limited DUT documentation is available.

    1. Study the circuit cards, looking for common components and circuits, and identify highlevel test points in the system and check for the presence or absence of fundamental signals. As before, start at one point and work your way backwards probing the major input and output signals at major nodes in the system.
    2. Compare waveforms at key nodes while changing the operating modes to see if a failure occurs. Store these waveforms.
    3. If an examination of the DUT and analysis of waveforms at key circuit nodes reveal no obvious faults, use the DSO’s storage capability to solicit the aid of peers.

• Identify “suspect” waveforms from the DUT.

• Use the DSO’s Extract or Output mode to save these waveform files in a bitmap (.bmp) format.

• Email the files to a peer or factory expert anywhere in the world for aid in troubleshooting the circuit.

 

    4. Using outside experts, go through each key node and one by one eliminate the obvious good nodes, eventually narrowing your focus to obvious faulty or suspect nodes.

Complete Selection of Fluke 120 Series ScopeMeters
Complete Selection of Fluke 190-Series ScopeMeter Oscilloscopes

View original article.

Published with permission from Fluke


Need someone to do your dirty work? Outsource your chemical blending to us!

February 15, 2010

Custom-Blended Chemicals

custom blending servicesMixing chemicals, especially for standard formulations, can add hours to the research and production process. Cole-Parmer provides a solution that saves you time (and costs) by eliminating this step—enabling chemists and related personnel to concentrate on other crucial tasks.

By using our custom-blending services for chemicals, you not only enhance your efficiency, you also ensure consistent quality guaranteed from batch to batch. Additionally, you improve safety within your facility by reducing the risk of chemical spills.

From 500 mL to 200 L, we can formulate and blend any combination of chemicals to your specifications. Whether you require a simple dilution or multiple chemicals in one solution, Cole-Parmer can respond to your needs. We can also supply your custom-blended chemicals in a specified container. To ensure quality, our custom-blended chemicals arrive at your facility with a Certificate of Analysis.

For more information on
custom-blending services, call
our Application Specialists at
800-323-4340.

View the original article.


Need to filter some fluid? Check out our Basics on Cartridge Filtration. Oh yeah!

February 12, 2010

Basics of Cartridge Filtration

Reasons for Filtration

Removal of Fluid Contaminants.
A properly designed cartridge filter system can eliminate many costly problems. The removal of contaminants from a fluid process stream makes that fluid more valuable and increases product yields. A dirty fluid stream can decrease productivity and lead to high rejection rates. A cartridge filter placed in a strategic location can alleviate such problems and also act as a monitor for the whole process. For example, a filter that plugs prematurely for no apparent reason suggests that there are improper conditions somewhere in the process. Cartridge filters can be used to protect critical orifices (i.e. an extruder) so that the openings do not become clogged and cause downtime. If the fluid in question is recirculating, reclaim value can also be increased by placing a cartridge filter in line. Removing a haze or classifying particles are other reasons for using cartridge filters. Properly dispersing a mixture, such as pigment/resin mixture, is an example of this.

Collection of Suspended Solids.
Many chemical processes require the use of catalysts in order to be functional. Cartridge filtration can recover the unused portions of the catalyst for reuse. If the catalyst is a precious metal, or if a precious metal is used in the actual reaction, cartridge filtration can recover unused portions and help reduce operating costs. In pollution control, contaminant’s need to be recovered from waste effluents before the fluid is released into the environment. This can be accomplished by cartridge filtration.

Means of Retention

Mechanical Retention
Mechanical retention occurs when a particle is mechanically restricted from passing through the filter medium. Direct interception, sieving, and bridging are mechanisms of capture that facilitate mechanical retention. Sieving is the most dependable under normal forward flow conditions. Particles captured by both bridging and direct interception are mechanically retained, but are more condition dependent than sieving. Pulsing or surging will dislodge a filter cake and/or small particles directly intercepted by media obstructions. However, if operating conditions are stable, particles held by mechanical retention should not be released.

Adsorptive Retention
Adsorptive retention refers to the adherence of a particle to the filter medium due to interactions between the particle and the surface of the medium. The particle “sticks” to the filter. Phenomena behind this adsorptive affect include electrical and hydrophobic interactions. Smaller particles adsorb more strongly than larger particles. The tendency of particles to adsorb, however, is very condition dependent. Adsorptive retention predominates for particles captured by inertial impaction, diffusion interception, and electro kinetic attraction.

Depth Filtration
The term “depth filtration” describes parameters of the particle size/pore size relationship present during the filtration process. Surface filters retain particles on the surface of the medium, where as depth filters retain particles throughout the medium. Although filters are often generalized as being depth filters, in reality, the label is inappropriate unless the particle size/pore size relationship is known.

Surface Filtration
A true surface filter can be thought of as a screen that is challenged with particles too large to pass through its openings. The particles will collect on the surface, forming a filter cake. Retention will be absolute since no particles will be able to penetrate through the surface. Note, however, that if the same screen was challenged with small enough particles, they will not be captured at the surface. Hence, the process of surface filtration is strictly dependent upon the particle size/pore size relationship.

Sieve Retention: Uniform Pore Size
Pleated filters are designed to enhance surface filtration when appropriately utilized. Micro-fiber sheet media has a narrow pore size distribution, favoring absolute sieving, in addition to a large surface area, increasing the capacity to retain particles at the surface. The medium is thin, permitting higher flows with lower pressure drops. These properties promote the formation of a filter cake, giving this type of filter a high dirt-holding capacity.

Published with permission from Pentair, Inc

View the original article.

Process Filtration Products
Big Blue Cartridge Filter System
Stainless Steel Multiple Filter Housings


Hey Genius, Take our Tech Challenge on Chemical Testing

February 5, 2010

Challenge: The U.S. EPA was testing rivers and lakes for chemical levels. The technician detected above-regulation levels in Lake Somhe, including phenol, toluene, mercury, oils, and more. There are a dozen different factories and pipelines which empty into Lake Somhe, and the EPA needs to determine which of these sources is contributing to the unacceptable chemical levels before doing a more in-depth analysis at the individual site.

The EPA contacted Cole-Parmer to find instruments or tests that can help them quickly and easily determine which sites are causing the problem.

Which test would be most effective for their purpose?

  1. Recommend a chemical classifier which work similar to a pH paper strip.
  2. Suggest the technician start with a colorimeter to determine phenol and toluene levels.
  3. Suggest a gas chromatograph and mass spectrophotometer to determine phenol and toluene levels.
  4. Have the EPA collect samples from each site and send to an independent testing laboratory.

See the answer.


Win a Bosch Tassimo Single-Serve Coffee Machine by spending $350!

February 5, 2010
You could win a Bosch TASSIMO Single-Serve Coffee Machine,
plus Two Packs of Starbucks® Coffee T-discs!
Orders over $350 placed online are automatically entered in our drawing without any further action or information required.
This contest runs from 2/1/2010 thru 2/28/2010.
win a coffee machine
If you wish to enter without purchasing, you may do so by sending a postcard to: Coffee Machine February 2010 Offer, c/o Cole-Parmer, eBusiness Department, 625 East Bunker Court, Vernon Hills, IL 60061 USA. On the postcard include: the date of mailing, your first and last name, company name, full shipping address, phone number and e-mail address. 

Bosch TASSIMO Single-Serve Coffee Machine features:

  • Single-serve coffee brewer brews at the touch of a button in about a minute
  • Uses T-Discs with barcode technology; beverages pour directly from T-Disc into cup
  • No measuring, no fuss, and virtually no cleanup; customizable size and strength

Terms and conditions


Artificial Heart Valve at the Museum of Science and Industry in Chicago Supported by Cole-Parmer Products

February 3, 2010
B/T pump
Photos: J.B. Spector / Museum of Science + Industry.

Exploring the heart is a compelling venture. For those touring the “YOU! The Experience” exhibit at the Museum of Science and Industry in Chicago, Illinois, the pumping artificial heart valve fascinates audiences, with its intricacy and functionality, in the exhibit’s Medical Innovations Gallery that is part of the 15,000-square feet of activities, challenges, and artifacts on human health and wellness.

Within the display, called “High-tech Human”, an Ismatec pump (available from Cole-Parmer) sends fluid through Cole-Parmer® tubing into a chamber that houses a bioengineered heart valve. The action of the pump keeps the fluid flowing and causes the valve’s leaflets to open and close. The valve educates guests about the mechanics of this vital organ and, specifically, illustrates the scientific advances achieved in creating a new generation of replacement organs grown in the laboratory.

B/T pump Like the organ it simulates in the display, the Ismatec pump controller is known for its clockwork-like precision and performance. Its versatility enables it to be used in a variety of applications, including laboratory research, pharmaceutical processing, manufacturing, food and beverage processing, life sciences, chemistry, and more. As evidenced in the museum’s exhibit, the Ismatec pump often shows up in unexpected places. 

Cole-Parmer offers the complete product line of these Swiss-engineered pumps, ranging from compact multichannel styles to washdown process pumps to fixed-speed rack-mount pumps. The pumps vary according to flow range, number of channels, and speed. The programmable dispensing pumps excel in continuous pumping or dispensing in five modes. Remote control capabilities make Ismatec pumps ideal for lab automation.

Ismatec drives will accept either peristaltic or gear heads, which offer varying advantages depending on their application. Peristaltic pumping is noncontaminating—with fluid only contacting the tubing—and easy to clean. The gear type is smooth-flowing, and compatible with high system pressure uses. Tubing to complement the Ismatec pumps is also available from Cole-Parmer, in a variety of formulations and sizes to best suit specific applications.

From showcasing the innovative high-tech human heart in an educational exhibit to pumping medicine into vials to processing ingredients for next week’s dinner, the Ismatec pump just keeps flowing. To learn more about the YOU! The Experience exhibit, visit www.msichicago.org. To find out more about choosing an Ismatec pump system for your application, go to http://www.coleparmer.com/5637

See the full article here:http://www.coleparmer.com/techinfo/techinfo.asp?htmlfile=IsmatecPump.htm&ID=1162&referred_id=5618


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