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An electron zap turns flimsy plastic into sturdy shrink wrap

Posted by Cole-Parmer on March 10, 2010

If you bought a Butterball turkey this Thanksgiving, you have particle accelerators to thank for its freshness. For decades now the food industry has used particle accelerators to produce the sturdy, heat-shrinkable film that Butterballs come wrapped in.

“Particle accelerators tie the molecules of plastic together and make the film tougher mechanically. It doesn’t crack or tear,” says Marshall Cleland, a technical advisor at IBA Industrial, an international company that has been manufacturing particle accelerators for commercial use since 1988.

Understanding how accelerators give cross-linked shrink film its unique properties requires a refresher course in chemistry.

Heat-shrinkable film—commonly known as shrink wrap—is made of polyethylene plastic. The plastic molecules, called polymers, are long chains of carbon atoms strung together like pearls. Each carbon atom also connects with two hydrogen atoms, leaving it no room to bond with anything else.

“The fully saturated carbon had its full meal, including dessert, and becomes chemically inert,” Cleland says. “If you heat it to the boiling point of water, it will turn into a syrupy mess.”

However, when hit with a beam of electrons from a particle accelerator, the plastic’s polymer strings become chemically active.

The electron beam knocks hydrogen atoms off the polymer chains, leaving the polymers hungry to fill those vacancies. If conditions are right, the carbon atoms in one chain bond with carbons in neighboring chains—and those carbon-carbon bonds are incredibly strong.

“The whole thing starts to knit together. Instead of being loose threads, it is sort of like a fishnet where everything is tied together,” Cleland says. “It is what we call a cross-linking reaction.”

When fully cross-linked, the plastic “becomes elastic if you heat it to boiling temperature, but it won’t melt,” Cleland says. After electron-beam treatment, the plastic is stronger and more heatresistant. It can be heated and stretched into a thin film without ripping. When cooled to room temperature, the cross-linked plastic retains its expanded shape. Place something inside it, such as a Butterball turkey, and apply heat, and the plastic shrinks back down to its original size, resulting in an air-tight wrapping.

The food industry purchases these cross-linked products from plastic manufacturers in large rolls or bags, depending on how the film will be used. You will find cross-linked shrink film wrapped around many items in the grocery store, such as turkeys, produce, and baked goods, as well as around board games, video games, DVDs, and CDs. “It’s a big business,” Cleland says.

Complete Selection of Chemical Property Testing

Published with permission from Symmetry Magazine, A joint Fermilab/SLAC publication

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Sound Measurement for Noise Ordinance Enforcement

Posted by Cole-Parmer on March 3, 2010

INTRODUCTION
The purpose of this application note is to provide basic instruction in the fundamentals of sound measurement to aid in the successful enforcement of noise ordinances. The main topics to be covered are sound and its characteristics and how they relate to the sound level meter.

Quest Technologies® NoisePro Personal Dosimeter DL

Quest Technologies® NoisePro Personal Dosimeter DL

SOUND DEFINED
When you blow up a balloon you are using your lungs to force air into the balloon. This causes the balloon skin to expand into its stretched out shape. The air in the balloon is now under pressure. If we squeeze the balloon in the middle, what happens? The balloon bulges out at the ends and the pressure inside the balloon increases. When the balloon is released it pops back to its original shape at its original pressure.

Suppose the balloon were very long and someone squeezed it at one end. What would we observe at the other end? First we would notice that nothing happened for a short period after it was first squeezed, then, just like the small balloon, the pressure would increase. What is happening is that the excess pressure caused by the squeeze is traveling down the tube at a speed of about 1200 feet per second. This excess pressure is the sound wave. If the squeeze were released, a decrease in pressure would travel down the tube in the same manner. To convince your self that these actions actually produce sound waves, burst the balloon with a pin.

How do we describe sound? Consider something that appears not to have anything to do with sound at all: a weight hanging from a spring.

If we pull the weight down a certain distance from the point it naturally hangs, then release it, the weight starts returning toward the rest position. But it goes through the rest position until it reaches a point as high above the rest position as it was pulled below it. The weight then starts down again to a new lowest position, where the process repeats over and over. Since the energy source of the person that initially pulled down on the weight is gone, the weight rises and falls a smaller distance each time, eventually coming to rest once again. The maximum displacement from the “at-rest” position is called the amplitude, and the time it takes to go through one complete cycle (from down to up to down) is called the period of the vibration. The number of periods that occur in one second is called the frequency. The units of frequency were once called cycles per second, but are now called Hertz and abbreviated “Hz”. So what’s the correlation between a weight on a spring and sound in air? Look at a stereo speaker emitting a single tone. As the speaker cone moves forward and backward like the spring, it alternately compresses and expands the air in front of the cone. The compression and expansion then moves out away from the speaker as a sound wave.

Single Frequency Sound
There are a number of common sources of sound that act much like the spring because they cause a single frequency sound to be produced. The keys of a piano are a good example. Pressing the middle C key causes its string to vibrate about 260 times per second. The vibrating string and soundboard cause the air adjacent to it to compress and expand with the same frequency. Just like the balloon, the changing pressure moves outward as a sound wave. Other examples of tones are the hum of a motor (60 Hz) and the sound of a police whistle (3500 Hz).

Random Motion–Noise
Suppose instead of just pulling the spring down and releasing it, there is an invisible hand that randomly either pulls or pushes on the weight at different times. Sound can behave in this random manner as well – think of music. So how would you describe this motion? Certainly there is no single frequency or amplitude with which to describe the motion as in the previous case. Fortunately noise such as this can be shown to consist of many single frequency components, each having its own amplitude.

Sound With Many Frequency Components
As an example of sound with many frequency components, consider motorcycles and automobiles. The amplitude of sound from motorcycles is typically greater than for automobiles. Motorcycle sound also contains components that are higher in frequency than an automobile. These are two reasons why motorcycles annoy people more than automobiles.

The Decibel
How do we describe the volume of sound we hear in everyday life? Because the sound levels we encounter in daily life can vary over such a wide range, talking about sound pressure in units such as pounds per square inch would be unwieldy. To remedy this situation we define Sound Pressure Level (SPL) as:

SPL = 20 x logarithm10 (measured sound pressure / reference sound pressure)

The reference pressure used for environmental noise turns out to be the lowest level sound that a person with normal hearing can detect. The unit of SPL is called the decibel (dB). Does all this complicated jargon mean that an enforcement officer will have to have a degree in mathematics? NO! All enforcement equipment is calibrated directly in decibels, so no calculations are involved.

Sound Level And Distance From The Source
Most people know that noise levels increase as you get closer to a sound source and decrease as you move away. It is important to note that the sound pressure level rises at a faster rate as you move closer and at a slower rate as you move away. Think about what happens when you drop a stone in water. The waves that are created are closer together and higher (amplitude) nearer the point of impact and further apart and lower as you move away from where the stone entered the water. Sound pressure behaves in the same manner. The importance of this observation is that officers should make sure he/she is at least as far away from the source as your ordinance requires when taking sound measurements. It is better to be a little too far than a little too close.

Combining Sound Pressure Levels
Suppose we have two identical sound sources, each alone producing the same dB level. So what is the SPL of the combined sources? It is not the sum of the two. We cannot simply add decibels directly to get the overall effect. The correct answer is obtained by using the following rule: Each time the number of identical noise sources is doubled, the SPL increases by 3dB; each time the number is halved, the SPL is decreased by 3dB. This rule is called 3dB doubling or 3dB exchange rate.

How does the 3dB rule help you? Suppose your noise ordinance has an 80dB noise limit. You cite a violator for causing an 89dB noise level and the case comes to court. The judge asks you how loud 89 dB is. Knowing this rule of thumb, you are able to tell the judge that 89 dB is the same noise level that would be generated by 8 identical vehicles, each producing the maximum allowable sound level of 80 dB. Case closed!! Be sure to apply the doubling rule contained in your particular ordinance.

Effects Of Additional Noise Sources
A third factor to remember when measuring sound involves the contribution to the overall level of all the other noise sources present at the time a violator is cited. This extraneous noise is called the ambient level. The violator might ask, “There were a number of other loud noise sources present when you cited me, so how do you know that they didn’t cause the readings to be too high?” The rule that applies here is: a violator should not be cited unless the level measured when the violation occurs is at least 10dB above the ambient noise level immediately before the violation. If this condition is met, then the additional noise caused by all the other sources producing noise will add less than 0.4dB to the level produced by the violator.

Sound Reflection
The last factor to remember is the effect of large objects on sound reflection. Think of the stone in the water again. If the water waves encounter an obstacle as they move away from where the stone entered the water, you will see part of the wave reflected back in the direction it came from, modifying the height of the waves, which is equivalent to the sound pressure in air. The same phenomenon occurs in air when measuring sound. The rule of thumb is to remain at least as far away from any large reflecting objects as you are from the source being measured. What about reflection from the ground? The noise level limit stated in the ordinance should take into account the fact that the noise heard by the receiver consists of sound that is reflected from the ground to the receiver as well as the direct wave. Normally there should be no concern. The exception is when the sound level meter is close to the ground. All measurements should be made with the microphone at least three feet above the ground.

The Sound Level Meter

The most common device used in noise ordinance enforcement is the sound level meter (SLM). The SLM performs three basic operations. It uses a microphone to convert the energy in the sound into an electrical signal. An electronic circuit then conditions the signal to provide meaningful results. Finally, the SLM communicates the results to the operator in one or more ways.

Before we address the specifics of various kinds of meters, we should address the most basic question of all, “How should I hold the SLM?” Should the microphone be pointed at the noise source or should the face of the microphone be oriented at some other angle such as at a right angle to the sound wave? The answer depends on the type of microphone being used. There are three different types of microphones available: free-field, random incidence and pressure. Free-field microphones should typically be pointed directly towards the noise source. Random incidence microphones should typically be held at a 70° angle to the source. Pressure microphones should typically be held at a right angle to the noise source. The rule here is to follow the manufacturer’s recommendations with respect to microphone orientation. Generally, low frequency sounds are not affected by the microphone orientation as much as high frequency sounds. Again, this depends largely upon what type of microphone element is used in the SLM.

The Basic SLM
Features vary considerably from meter to meter and from manufacturer to manufacturer. Perhaps surprisingly, so can performance and accuracy. No matter what type of SLM is used, at least two requirements of the meter should always be met. These include some method for performing a field calibration of the SLM and an independent certification that the SLM meets Type I or Type II standards of performance and all other applicable SLM standards in your locality. Your noise ordinance should include a statement of standards that must be met by the meter.

In its most basic form, the SLM will provide the operator with an indication of the instantaneous SPL being detected. Often a basic meter will also provide an indication of the maximum SPL encountered as well. Results from a Basic SLM’s are almost certainly limited to presentation through the display of the meter. Rarely are there capabilities for these meters to output results to a printer or computer. There may or may not be provisions in the meter to allow the operator to change certain characteristics of the SLM’s signal conditioning circuits. These characteristics in a basic meter may or may not include the weighting network and the response time constant. Your noise ordinance should include a specification as to which weighting network and response time constant is to be used.

Weighting networks most common today consist of “A”, “C” and “Z” weighting. Each of these weighting networks is a “standard” that dictates how the SLM will recognize the amplitude of the SPL based on the frequency of the sound. For instance, “A” weighting circuits simulate how the human ear responds to sound. We know that humans can hear within a fixed range of frequencies and humans perceive that sound is louder or softer as frequency changes.

Response time constants define how quickly an instrument must be able to recognize and process changing SPL’s. The most common options today are “Fast”, “Slow”, “Peak” and “Impulse” time constants. If it were not for the existence of frequency weighting and response time constant standards, results from meter to meter and manufacturer to manufacturer would almost certainly vary widely and prohibit the effective measurement and enforcement of noise limits.

Integrating SLM’s
Depending upon the requirements of your noise ordinance, you may need an SLM that computes the average SPL over a prescribed amount of time. These types of SLM’s are referred to as Integrating SLM’s because they automatically calculate the average SPL. All Integrating SLM’s calculate this result based on a given doubling or exchange rate, as discussed earlier. Some SLM’s may be fixed for a specific exchange rate at the factory. Others may include provisions for setting the exchange rate in the field. In either event, it is important to note which exchange rate the SLM is using and that it matches the requirements of your noise ordinance. Since it is possible for ordinances to change, it is always more favorable to have an SLM that allows the exchange rate to be changed by the user without requiring factory modification, or worse yet, replacement. Integrating SLM’s may include provisions for printing results or uploading them to computer. Generally speaking, unless the meter also documents the performance of a field calibration in its output, the value of the hard copy results is greatly diminished.

Datalogging SLM’s
After integration, the next mostly commonly sought after capability in an SLM is datalogging. Datalogging SLM’s provide much more detail of the noise-testing event. This can include a minute-by-minute profile of the sound source’s SPL levels. At a minimum, these kinds of meters should provide hard-copy and computer upload of test results correlated to the real-time and date of the event.

Octave Band SLM’s and Real Time Analyzers
At the top end of the spectrum for SLM’s you will find devices that are capable of determining and reporting the SPL and average SPL at various frequencies. These meters are rarely used for noise ordinance enforcement since ordinances rarely specify noise limits as a function of frequency. Generally speaking, once frequency content of the sound is a concern, specialists in acoustics are required to perform these tests.

Complete Selection of Quest Cable-Free Noise Dosimeters
Complete Selection of Quest SoundPro Sound Level Meters
Complete Selection of Quest Technologies Integrating Sound Meters with RS-232
Complete Selection of Quest Technologies Intrinsically Safe Sound Meters
Complete Selection of Quest Technologies NoisePro Personal Dosimeters

Published with permission from Quest Technologies

Full article can be found at:  http://www.coleparmer.com/techinfo/techinfo.asp?htmlfile=Sound_Measurement.htm&ID=1183&referred_id=5618

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Temperature Calibration in Industrial Processes. Woo-hoo!

Posted by Cole-Parmer on February 19, 2010

 

Temperature is one of the most frequently measured parameters in industrial processes. A wide variety of mechanical and electrical thermometers are used to sense and control process temperatures. Regular calibration of these thermometers is critical to ensuring consistent quality of product manufactured, as well as providing regulatory compliance for some industries.

 

The Basics

Most simply stated, temperature calibration consists of placing a thermometer under test into a known, stable temperature environment. A comparison is made between the actual temperature and the reading indicated by the thermometer under test and the difference is noted.

Adjustments can then be made either directly to the thermometer or to its readout. Electrical thermometers are adjusted by mathematically re-creating the coefficients used by SMART transmitters or other readout devices to translate their electrical output to temperature. Many mechanical thermometers, such as dial gauges can be adjusted by turning a dial or other mechanical device. In some cases, such as liquid-in-glass thermometers, direct adjustments are not possible and offsets must be noted.

In industrial applications, the temperature environment is usually provided by a drywell, or “dry-block” calibrator, or a micro-bath. Both offer portability and a wide range of temperatures. Drywells use high stability metal blocks with drilled wells to accept the reference and UUT. Drywells typically cover ranges from -45°C to 1200°C and micro-baths cover ranges from -25°C to 200°C. Micro-baths are similar in size to drywells but use a small tank of stirred fluid instead of a metal block. Micro-baths offer significant advantages when calibrating short or odd shaped probes.

The “actual” temperature of the bath or dry-well is determined by a reference thermometer, which may be either a thermometer internal to the heat source or an external reference thermometer operating independent of the heat source.

Figure 1: Heat source as reference standard

External or Internal Reference

Micro-baths and dry-wells have a built-in sensor to provide a feedback loop to the unit’s controller and to provide a temperature reading to the user. The manufacturer of the heat source (or a third-party laboratory) can calibrate this sensor so the unit displays a traceable temperature within a stated uncertainty. For some applications, this uncertainty level (typically ±1-2°F) is adequate. Using an internal reference is sometimes preferred because it requires fewer instruments and enhances portability for field applications. This method is illustrated in Figure 1.

The reference system, however, should be more accurate than the process system being calibrated. The generally accepted Test Uncertainty Ratio (TUR) is 4:1 (i.e. the reference should be four times more accurate than the sensor or system being calibrated). Therefore, if a process thermometer is being relied on for correct readings within ±2°F, the test system should typically be ±0.5°F or better at each temperature in question. As a general rule, temperature uncertainties are larger at higher temperatures.

Figure 2: External reference standard

Where uncertainty requirements are more rigorous, external reference thermometers help improve system uncertainty (see Figure 2). These thermometers—usually platinum resistance thermometers (PRTs) or thermistors—can often be calibrated to a few hundredths of a degree and can be read by electronic readout devices that contribute little to total measurement uncertainty. These systems can provide measurements with uncertainties as low as ±0.05°F or ±0.02°F—or better. The reference probe and readout should be periodically re-calibrated, preferably by an accredited cal lab, to assure performance specifications and maintain traceability.

Because external thermometers are more accurate, they increase the relative significance of other components of calibrations uncertainty, such as uniformity and stability. It is, of course, critical in any calibration to account for all sources of uncertainty in the process.

System or Component Calibrations

Most temperature sensors used in processes are read by transmitters, which send a 4 to 20 mA signal to a control panel, which then displays the temperature for process monitoring. Such systems involve three instruments, all of which require periodic calibration. Of these three, the largest errors are often found in the temperature sensor (which is subject to drift for a variety of reasons), so its calibration is of particular concern.

More Details
or Order Online:

Hart Scientific Field Temperature Dry Wells

High-Temperature Field Dry Block Calibrator

Industrial Dual-Block Calibrator

Several calibration methodologies are used in the process plant with the most representative method being to calibrate the complete measurement system from sensor through transmitter to indicator or controller; alternatively each component of the measurement system can be individually calibrated.

The temperature sensor can be individually calibrated using a drywell or micro-bath heat source to simulate the process temperature. If the temperature sensor is electrical, a readout device measures its output. Adjustments are then made to the thermometer or its coefficients as discussed earlier.

The transmitter is calibrated using a precision simulator to generate the resistance or voltage output from the temperature sensor and input to the transmitter. The simulator also measures the resulting transmitter current or voltage output. The transmitter is adjusted to ensure that the output follows the input, e.g. for a 4 to 20 mA transmitter with a range of 0°C to 200°C, 4 mA corresponds to 0°C and 20 mA corresponds to 200°C. The simulator provides a wide range of input and output ranges to cover all resistance thermometer and thermocouple types.

The indicator or controller is also calibrated using a precision simulator to generate simulate the resistance or current input from the transmitter. The indicator or controller is adjusted so that the display variable matches the simulated input.

The complete system is calibrated using the drywell or micro-bath to compare the reference probe and UUT. The transmitter is adjusted to ensure that the indicator or controller agrees with the reference probe readout. This calibration method is most representative of the real process, is faster and simpler to perform.

Accredited Calibration Services

Calibration of the thermometer standards used to calibrate industrial thermometers provides traceability, which means that measurements are traceable to national and international standards. Traceability to international standards ensures that measurements made in one country agree with measurements in another country, which is particularly important for companies using similar manufacturing processes at different locations around the world.

More Details
or Order Online:

InnoCal Calibration Services

More and more calibration labs throughout the U.S. are being accredited to international standards such as the ISO Guide 25. Accreditation ensures that a lab’s quality systems, uncertainty levels, and traceability statements have been examined and independently verified. NVLAP and A2LA are the primary accrediting bodies in the U.S. A recently signed international agreement ensures that accrediting bodies in almost every developed nation also recognize accreditations granted by NVLAP and A2LA.

In summary, process plant temperature calibrations require a good reference thermometer with readout, a drywell and/or micro-bath heat source, and a precision simulator. These instruments, in turn, should be periodically calibrated by a reputable lab, preferably one that is accredited and can prove traceability.

How to Determine Thermocouple System Accuracy
Temperature Controller Features
Temperature Conversion Equations
Temperature Instrument Ranges

View original article.

by Bernard Morris, Vice-President of Sales, Hart Scientific, Inc.
Reprinted with permission of Hart Scientific, Inc.

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Want to measure some voltage? Read our intro on Oscilloscopes.

Posted by Cole-Parmer on February 17, 2010

This introduction to digital storage oscilloscopes (DSOs)
takes you on a quick but comprehensive tour of DSO
functions and measurements.

An oscilloscope measures and displays voltage signals on a time-versus-voltage graph. In most applications the graph shows how the signal changes over time: the vertical (Y) axis represents voltage, and the horizontal (X) axis represents time. This simple graph can tell you many things about a signal:

    • View the signal for glitches.
    • Calculate the frequency of an oscillating signal.
    • Tell if a malfunctioning component is distorting the signal.
    • Tell how much of the signal is noise and whether the noise is changing with time.

Today’s handheld digital storage oscilloscopes offer two critical advantages over benchtop models: they are battery-operated, and they use isolated, electrically floating inputs. These designs make safety-certified measurements possible in 1000V CAT II and 600V CAT III environments — a critical need for safely troubleshooting electrical devices in high-energy applications.

Scopemeters Far left: The Fluke 190 Series ScopeMeter has a 200 MHz bandwidth and 2.5 GS/s real-time sampling rate.

Left: The Fluke 123 ScopeMeter with 20 MHz dual-input measurement shows both meter reading and waveform.

Time/Volt/Graph Figure 1. Time-versus-voltage graph.

Scopes and DMMs
The difference between an oscilloscope and a DMM (digital multimeter) can be summarily stated as “pictures vs. numbers.” A DMM is a tool for making precise measurements of discrete signals, enabling readings of up to eight digits of resolution for the voltage, current or frequency of a signal. On the other hand, it cannot depict waveforms visually to reveal signal strength, waveshape, or the instantaneous value of the signal. Nor is it equipped to reveal a transient or a harmonic signal that could compromise the operation of a system.

A scope adds a wealth of information to the numeric readings of a DMM. While displaying instantaneous numerical values of a wave, it also reveals the shape of the wave, including its amplitude (voltage) and frequency. With such visual information, a transient signal that may pose major consequences to a system can be displayed, measured and isolated.

Reach for a scope if you want to make both quantitative and qualitative measurements. Use a DMM to make high-precision checks of voltage, current, resistance and other electrical parameters.

Sampling
Sampling is the process of converting a portion of an input signal into a number of discrete electrical values for the purpose of storage, processing and display. The magnitude of each sampled point is equal to the amplitude of the input signal at the time the signal is sampled. The input waveform appears as a series of dots on the display. If the dots are widely spaced and difficult to interpret as a waveform, they can be connected using a process called interpolation, which connects the dots with lines, or vectors.

Triggering
Trigger controls allow you to stabilize and display a repetitive waveform.

Edge triggering is the most common form of triggering. In this mode, the trigger level and slope controls provide the basic trigger point definition. The slope control determines whether the trigger point is on the rising or the falling edge of a signal, and the level control determines where on the edge the trigger point occurs.

For even greater control and visibility into signal phenomena, you can use the ability of some DSOs to capture events leading up to the trigger point (“pre-trigger”) or after the trigger point (“posttrigger”) on the input waveform. As one example, by using pretriggering or post-triggering, you may catch a spike that occurs in between two occurrences of a signal.

Pulse width triggering triggers on specific pulses within a series or it can identify one-time or sporadic problems in a pulsed signal. In this mode, you can monitor a signal indefinitely and trigger on the first occurrence of a pulse whose duration, or pulse width, is either outside of or within set limits. The goal is to isolate and display a pulse that meets the predetermined time criteria.

Single-shot triggering is useful for capturing a one-time event — such as electrical arcing or a relay closure. A DSO with a single-shot mode waits until it receives a trigger and then sets itself in a hold mode to store the signal at the moment the onetime event occurs.

Video triggering is a powerful feature of advanced DSOs. Video signals can be extremely complex, providing no unique edge that is repetitive and that can be isolated to stabilize the signal. With an extensive range of signaling protocols in use in today’s electronicvideo equipment and systems, an effective DSO is one that recognizes the predominant video protocols and provides appropriate triggering functionality.

Sampling Graph Figure 2. Sampling and interpolation.

Setup The task of capturing and analyzing an unknown waveform on an oscilloscope can be routine, or it can seem like taking a shot in the dark. However, in most cases, taking a methodical approach to setting the oscilloscope will capture a stable waveform or help you determine how the scope controls need to be set so that you can capture the waveform.

1) Start with Auto Connect the ground reference lead and then connect the probe tip to the circuit test point. Most oscilloscopes have the ability to either perform a one-time auto setup or continuously analyze the unknown input signal. Press the AUTO button or verify that the scope is already in Auto mode.

Pressing the AUTO button will typically set up the oscilloscope to automatically adjust three key parameters:

Vertical sensitivity. Adjusts the vertical sensitivity so that the vertical amplitude spans approximately three to six divisions.

3-6 Vert Graph Figure 3. Unknown trace adjusted for 3-6 vertical divisions.

Horizontal timing. Adjusts the horizontal time per division so that there are three to four periods of the waveform across the width of the display.

3-4 Horizontal Graph Figure 4. Unknown trace adjusted for 3-4 periods horizontally.

Trigger position. Sets the trigger position to the 50 % point of the vertical amplitude. Depending on the signal characteristics, this action may or may not result in a stable display.

Trigger Point Figure 5a. Trigger point set to 50% point on trace.

Trigger Second Period Figure 5b. Trigger point is set to the 50 % point but due to the aberration on the leading edge in the second period, an additional trigger results in an unstable display.

At this point you should see a trace that 1) lies within the vertical range of the display, 2) shows at least three periods of a waveform, and 3) is stable enough to allow you to recognize the overall characteristics of the waveform. Next, start fine-tuning the settings.

2) Adjust vertical and horizontal settings Start by adjusting the horizontal timing, increasing the time per division so that you see a wide time span of the unknown waveform. From that view, reverse the adjustment as required to narrow the view to just what you want to display.

Now adjust the vertical sensitivity, expanding the waveform vertically but ensuring that the high and low points of the waveform do not exceed the vertical span.

3) Adjust trigger settings If needed, adjust the trigger settings to stabilize the waveform display. Or, you may want to adjust the trigger delay to see pre- or post-trigger details on the waveform. Always start with the trigger-level setting, adjusting it so that it falls on a repetitive, unique point on the rising or falling edge of a waveform.

As an example, with the oscilloscope trigger set to the rising edge and the level set to the 50 % point, the following figures illustrate the cause of an unstable waveform display.

First Trig Point Figure 6a. At the first update, the scope triggers on the first edge. On the second update, the scope may trigger on the second trigger point indicated.

After two successive updates based on triggers 1 and 2, the resultant trace will appear unstable.

Unstable Wave Figure 6b. Unstable waveform display caused by incorrect trigger level setting.

However, simply by manually adjusting the trigger point to a repetitive, unique point on the edge, you can solve this problem and produce a stable waveform display.

Repetitive Graph Figure 6c. Trigger level adjusted to a unique repetitive position, outside the aberration on the second period.

When working with complex signals like a series of pulses, pulse width triggering may be required. With this technique, both the trigger-level setting and the next falling edge of the signal must occur within a specified time span. Once these two conditions are met, the oscilloscope triggers.

Specific Pulse Figure 7. Pulse width triggering will allow you to set up the oscilloscope to trigger on a specific pulse defined by level and time.

Another technique is singleshot triggering, by which the oscilloscope will display a trace only when the input signal meets the set trigger conditions. Once the trigger conditions are met, the oscilloscope acquires and updates the display, and then freezes the display to hold the trace.

Understanding and reading waveforms
The majority of electronic waveforms encountered are periodic and repetitive, and they conform to a known shape. Here are the factors to consider in analyzing waveforms:

Shape. Repetitive waveforms should be symmetrical. That is, if you were to print the traces and cut them in two like-sized pieces, the two sides should be identical. A point of difference could indicate a problem.

Non Symmetrical Grph Figure 8. If the two components of the waveform are not symmetrical, there may be a problem with the signal.

Rising and falling edges. Particularly with square waves and pulses, the rising or falling edges of the waveform can greatly affect the timing in digital circuits. It may be necessary to decrease the time per division to see the edge with greater resolution.

Cursors/Graticule Figure 9. Use cursors and the graticule marks to evaluate the rise and fall times of the leading and trailing edges of a waveform.

Amplitude. Verify that the level is within the operating specifications of the circuit. Also check for consistency, from one period to the next. Monitor the waveform for an extended period of time, watching for any changes in amplitude.

Horizontal Cursors Figure 10. Use horizontal cursors to identify amplitude fluctuations.

Amplitude offsets. DC-couple the input and determine where the ground reference marker is. Evaluate any DC offset and observe if this offset remains stable or fluctuates.

DC Offsets Figure 11. Evaluate waveform DC offsets.

Periodic waveshape. Oscillators and other circuits will produce waveforms with constant repeating periods. Evaluate each period in time using cursors to spot inconsistencies.

Period/Period Figure 12. Evaluate period-to-period time changes.

Waveform anomalies Here are typical anomalies that may appear on a waveform, along with the typical sources of such anomalies.

Transients or glitches. When waveforms are derived from active devices such as transistors or switches, transients or other anomalies can result from timing errors, propagation delays, bad contacts or other phenomena.

Transient Figure 13. A transient is occurring on the rising edge of a pulse.

Noise. Noise can be caused by faulty power supply circuits, circuit overdrive, crosstalk, or interference from adjacent cables. Or, noise can be induced externally from sources such as DC-DC converters, lighting systems and high-energy electrical circuits.

Ground Reference Figure 14. A ground reference-point measurement showing induced random noise.

Ringing.
Ringing can be seen mostly in digital circuits and in radar and pulse-width-modulation applications. Ringing shows up at the transition from a rising or falling edge to a flat DC level. Check for excessive ringing, adjusting the time base to give a clear depiction of the transitioning wave or pulse.

Excessive Ringing Figure 15. Excessive ringing occurring on the top of the square wave.

Momentary fluctuation. Momentary changes in the measured signal generally result from an external influence such as a sag or surge in the mains voltage, activation of a high-power device that is connected to the same electrical grid, or a loose connection. Use the DSO’s slowest timebase setting or the paperless recording or “roll” mode. Start at the input and watch the acquired waveform over long time spans to track down the source of the problem.

Momentary Change Figure 16a. A momentary change of approximately
1.5 cycles in the amplitude of the sinewave.
Plotting Amplitude Figure 16b. Using an oscilloscope with a paperless recorder mode allows plotting of the amplitude (voltage level) over time.

Drift. Drift — or minute changes in a signal’s voltage over time — can be tedious to diagnose. Often the change is so slow that it is difficult to detect. Temperature changes and aging can affect passive electronic components such as resistors, capacitors and crystal oscillators. One problematical fault to diagnose is drift in a reference DC voltage supply or oscillator circuit. Often the only solution is to monitor the measured value (V dc, Hz, etc.) over an extended time.

Freq. Measurement Figure 17. Performing a frequency measurement on a crystal oscillator that has been trend-plotted over an extended period (days or even weeks) can highlight the affect of drift caused by temperature changes and aging.

Diagnosing problems Although successful troubleshooting is both an art and a science, adopting a troubleshooting methodology and relying on the functionality of an advanced DSO can greatly simplify the process.

Good troubleshooting practices will save time and frustration. The time-tested approach known as KGU, Known Good Unit comparison, accomplishes both goals. KGU builds on a simple principle: an electronic system that is working properly exhibits predictable waveforms at critical nodes within its circuitry, and these waveforms can be captured and stored. This reference library can be stored right on the DSO as an online resource, or can be printed out to serve as a hardcopy reference document. If the system or an identical system later exhibits a fault or failure, waveforms can be captured from the faulty system — called the device under test (DUT) — and compared with their counterparts in the KGU. Consequently, the DUT can either be repaired or replaced.

To build a reference library, start by identifying appropriate test points, or nodes, on the DUT. Now, run the KGU through its paces, capturing the waveform from each node. Annotate each waveform as required.

Get into the habit of always documenting key waveforms and measurements. Having a reference to compare to will prove invaluable during future troubleshooting

Troubleshooting
Whichever troubleshooting scenario below is appropriate at the time, remember that it’s important to inspect waveforms for fast-moving transients or glitches, even if a spot check of the waveform reveals no anomalies. These events can be difficult to spot, but the high sampling rate of today’s DSOs, together with effective triggering, makes it possible.

DUT with KGU. This approach assumes that you have access to a KGU and a reference library.

    1. Make sure the DUT and KGU are set up in identical operating modes.
    2. Starting at a high-level point in the system or block diagram, use the DSO to look for the presence or absence of fundamental signals. For example, look for a line-voltage supply, as well as subsequent DC supply voltages to the various subsystems. This requires probing the major input and output signals at major nodes in the system.
    3. Compare signals at key nodes while changing the operating mode to see if a failure occurs. With signals from both devices available, you have two options:

• Display the live waveform from the KGU on Channel 1 of the DSO, and display the live waveform from the DUT on Channel 2.

• Capture a trace from the KGU and overlay it with a trace from the DUT. Perform a waveform-compare or pass/fail test.

    4. Continue with this process until you note a variance between the DUT and KGU waveforms.

DUT with Circuit Diagrams. This approach assumes that no KGU and no waveform reference library for the DUT are available, but that circuit diagrams of the DUT can be located.

    1. Review the circuit diagrams to understand the basic operation of the DUT.

• Analog circuits such as oscillators, amplifiers and signal conditioners (attenuators, filters and dividers) should exhibit uniform waveform patterns.

• Digital circuits such as gates, switches and processors should display waveforms with predictable amplitudes, pulse periods and even pulse patterns.

    2. Starting at a high-level point in the system or block diagram, use the DSO to look for the presence or absence of fundamental signals. For example, look for a line-voltage supply, as well as subsequent DC supply voltages to the various subsystems. This requires probing the major input and output signals at major nodes in the system.
    3. Use the storage capability of the DSO to capture and compare waveforms while changing the operating mode of the DUT.

• Visualize a theoretical “good” waveform and compare it to the waveform displayed on the DSO. Try to identify any obvious anomalies.

 

    4. Use the horizontal or vertical cursors to quickly evaluate if the time or amplitude of the trace falls within the time or amplitude ranges suggested by the circuit design.

Complex DUT, No Circuit Diagrams. This approach assumes that the DUT is a fairly complex system, that no KGU is available, and that only limited DUT documentation is available.

    1. Study the circuit cards, looking for common components and circuits, and identify highlevel test points in the system and check for the presence or absence of fundamental signals. As before, start at one point and work your way backwards probing the major input and output signals at major nodes in the system.
    2. Compare waveforms at key nodes while changing the operating modes to see if a failure occurs. Store these waveforms.
    3. If an examination of the DUT and analysis of waveforms at key circuit nodes reveal no obvious faults, use the DSO’s storage capability to solicit the aid of peers.

• Identify “suspect” waveforms from the DUT.

• Use the DSO’s Extract or Output mode to save these waveform files in a bitmap (.bmp) format.

• Email the files to a peer or factory expert anywhere in the world for aid in troubleshooting the circuit.

 

    4. Using outside experts, go through each key node and one by one eliminate the obvious good nodes, eventually narrowing your focus to obvious faulty or suspect nodes.

Complete Selection of Fluke 120 Series ScopeMeters
Complete Selection of Fluke 190-Series ScopeMeter Oscilloscopes

View original article.

Published with permission from Fluke

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Need someone to do your dirty work? Outsource your chemical blending to us!

Posted by Cole-Parmer on February 15, 2010

Custom-Blended Chemicals

custom blending servicesMixing chemicals, especially for standard formulations, can add hours to the research and production process. Cole-Parmer provides a solution that saves you time (and costs) by eliminating this step—enabling chemists and related personnel to concentrate on other crucial tasks.

By using our custom-blending services for chemicals, you not only enhance your efficiency, you also ensure consistent quality guaranteed from batch to batch. Additionally, you improve safety within your facility by reducing the risk of chemical spills.

From 500 mL to 200 L, we can formulate and blend any combination of chemicals to your specifications. Whether you require a simple dilution or multiple chemicals in one solution, Cole-Parmer can respond to your needs. We can also supply your custom-blended chemicals in a specified container. To ensure quality, our custom-blended chemicals arrive at your facility with a Certificate of Analysis.

For more information on
custom-blending services, call
our Application Specialists at
800-323-4340.

View the original article.

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Need to filter some fluid? Check out our Basics on Cartridge Filtration. Oh yeah!

Posted by Cole-Parmer on February 12, 2010

Basics of Cartridge Filtration

Reasons for Filtration

Removal of Fluid Contaminants.
A properly designed cartridge filter system can eliminate many costly problems. The removal of contaminants from a fluid process stream makes that fluid more valuable and increases product yields. A dirty fluid stream can decrease productivity and lead to high rejection rates. A cartridge filter placed in a strategic location can alleviate such problems and also act as a monitor for the whole process. For example, a filter that plugs prematurely for no apparent reason suggests that there are improper conditions somewhere in the process. Cartridge filters can be used to protect critical orifices (i.e. an extruder) so that the openings do not become clogged and cause downtime. If the fluid in question is recirculating, reclaim value can also be increased by placing a cartridge filter in line. Removing a haze or classifying particles are other reasons for using cartridge filters. Properly dispersing a mixture, such as pigment/resin mixture, is an example of this.

Collection of Suspended Solids.
Many chemical processes require the use of catalysts in order to be functional. Cartridge filtration can recover the unused portions of the catalyst for reuse. If the catalyst is a precious metal, or if a precious metal is used in the actual reaction, cartridge filtration can recover unused portions and help reduce operating costs. In pollution control, contaminant’s need to be recovered from waste effluents before the fluid is released into the environment. This can be accomplished by cartridge filtration.

Means of Retention

Mechanical Retention
Mechanical retention occurs when a particle is mechanically restricted from passing through the filter medium. Direct interception, sieving, and bridging are mechanisms of capture that facilitate mechanical retention. Sieving is the most dependable under normal forward flow conditions. Particles captured by both bridging and direct interception are mechanically retained, but are more condition dependent than sieving. Pulsing or surging will dislodge a filter cake and/or small particles directly intercepted by media obstructions. However, if operating conditions are stable, particles held by mechanical retention should not be released.

Adsorptive Retention
Adsorptive retention refers to the adherence of a particle to the filter medium due to interactions between the particle and the surface of the medium. The particle “sticks” to the filter. Phenomena behind this adsorptive affect include electrical and hydrophobic interactions. Smaller particles adsorb more strongly than larger particles. The tendency of particles to adsorb, however, is very condition dependent. Adsorptive retention predominates for particles captured by inertial impaction, diffusion interception, and electro kinetic attraction.

Depth Filtration
The term “depth filtration” describes parameters of the particle size/pore size relationship present during the filtration process. Surface filters retain particles on the surface of the medium, where as depth filters retain particles throughout the medium. Although filters are often generalized as being depth filters, in reality, the label is inappropriate unless the particle size/pore size relationship is known.

Surface Filtration
A true surface filter can be thought of as a screen that is challenged with particles too large to pass through its openings. The particles will collect on the surface, forming a filter cake. Retention will be absolute since no particles will be able to penetrate through the surface. Note, however, that if the same screen was challenged with small enough particles, they will not be captured at the surface. Hence, the process of surface filtration is strictly dependent upon the particle size/pore size relationship.

Sieve Retention: Uniform Pore Size
Pleated filters are designed to enhance surface filtration when appropriately utilized. Micro-fiber sheet media has a narrow pore size distribution, favoring absolute sieving, in addition to a large surface area, increasing the capacity to retain particles at the surface. The medium is thin, permitting higher flows with lower pressure drops. These properties promote the formation of a filter cake, giving this type of filter a high dirt-holding capacity.

Published with permission from Pentair, Inc

View the original article.

Process Filtration Products
Big Blue Cartridge Filter System
Stainless Steel Multiple Filter Housings

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Artificial Heart Valve at the Museum of Science and Industry in Chicago Supported by Cole-Parmer Products

Posted by Cole-Parmer on February 3, 2010

B/T pump
Photos: J.B. Spector / Museum of Science + Industry.

Exploring the heart is a compelling venture. For those touring the “YOU! The Experience” exhibit at the Museum of Science and Industry in Chicago, Illinois, the pumping artificial heart valve fascinates audiences, with its intricacy and functionality, in the exhibit’s Medical Innovations Gallery that is part of the 15,000-square feet of activities, challenges, and artifacts on human health and wellness.

Within the display, called “High-tech Human”, an Ismatec pump (available from Cole-Parmer) sends fluid through Cole-Parmer® tubing into a chamber that houses a bioengineered heart valve. The action of the pump keeps the fluid flowing and causes the valve’s leaflets to open and close. The valve educates guests about the mechanics of this vital organ and, specifically, illustrates the scientific advances achieved in creating a new generation of replacement organs grown in the laboratory.

B/T pump Like the organ it simulates in the display, the Ismatec pump controller is known for its clockwork-like precision and performance. Its versatility enables it to be used in a variety of applications, including laboratory research, pharmaceutical processing, manufacturing, food and beverage processing, life sciences, chemistry, and more. As evidenced in the museum’s exhibit, the Ismatec pump often shows up in unexpected places. 

Cole-Parmer offers the complete product line of these Swiss-engineered pumps, ranging from compact multichannel styles to washdown process pumps to fixed-speed rack-mount pumps. The pumps vary according to flow range, number of channels, and speed. The programmable dispensing pumps excel in continuous pumping or dispensing in five modes. Remote control capabilities make Ismatec pumps ideal for lab automation.

Ismatec drives will accept either peristaltic or gear heads, which offer varying advantages depending on their application. Peristaltic pumping is noncontaminating—with fluid only contacting the tubing—and easy to clean. The gear type is smooth-flowing, and compatible with high system pressure uses. Tubing to complement the Ismatec pumps is also available from Cole-Parmer, in a variety of formulations and sizes to best suit specific applications.

From showcasing the innovative high-tech human heart in an educational exhibit to pumping medicine into vials to processing ingredients for next week’s dinner, the Ismatec pump just keeps flowing. To learn more about the YOU! The Experience exhibit, visit www.msichicago.org. To find out more about choosing an Ismatec pump system for your application, go to http://www.coleparmer.com/5637

See the full article here:http://www.coleparmer.com/techinfo/techinfo.asp?htmlfile=IsmatecPump.htm&ID=1162&referred_id=5618

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Visit Cole-Parmer at the 61st Annual PITTCON® Conference in Sunny Orlando, Florida

Posted by Cole-Parmer on January 15, 2010

View the latest laboratory, life science, and industrial products at booth #2141 in the West Building of the Orange County Convention Center
 
Vernon Hills, Ill., January 11, 2010—Cole-Parmer, an exhibitor at the PITTCON Conference and Expo 2010, February 28–March 5 in Orlando, Florida, will showcase a selection of its lines of laboratory equipment, fluid handling products, temperature equipment, measurement instrumentation, electrochemistry instrumentation, and InnoCal® calibration services.Powerful new products will be on display, including, the Pro-Spense line of innovative syringe pumps, the Oakton® 700 series pH/dissolved oxygen benchtop meters, and the economical handheld digital USB microscopes.

This year also features a line of life science products including laboratory equipment and labware.In addition, other popular laboratory items such as the Masterflex® L/S® Digital Pump Drives and the Stir-Pak® General-Purpose Mixer will be highlighted at the event.

While visiting booth #2141, attendees can try many of these products, with experts available to respond to questions and provide demonstrations.

As an added bonus, visitors can log on to ColeParmer.com and check out the free support tools—such as Customer-Written Product Reviews, Technical Information, Live Chat, Answer Box, and more—created to make their jobs easier.

Cole-Parmer staff members will be standing by to help navigate and explore these handy tools.

Visitors may also register for a chance to win one of three Amazon Kindle® wireless reading devices, the number one best-selling, most wished-for gift on Amazon.com®.

For more information, call 800-323-4340 or visit ColeParmer.com

Cole-Parmer has been a leading global source of laboratory and industrial fluid handling products, instrumentation, equipment, and supplies since 1955.

Our product lines, including popular brand names such as Masterflex®, Oakton®, and more, are sold through company-owned customer channel outlets and a strong network of international dealers.

We also feature an ISO-17025-accredited metrology lab for instrument calibration and repair.

Cole-Parmer responds with excellence to customer needs, and offers application expertise and technical support. For more information, contact Cole-Parmer, 625 East Bunker Court, Vernon Hills, IL 60061.

In the U.S., call 800-323-4340. International customers, call 847-549-7600. Visit us at ColeParmer.com

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60 seconds to win an Amazon Kindle

Posted by Cole-Parmer on January 11, 2010

Each month through March 2010, Cole-Parmer will be giving away one Kindle Wireless Reading Device. To become eligible, simply complete one of the following:

  1. Update your account information (you must be logged in and go to myCP Account/myCP profile).
  2. Please register, if you’re not already a registered account holder with Cole-Parmer.

In return you will be automatically entered in our monthly drawing for a FREE Kindle Wireless Reading Device.

 One Kindle will be given away each month through March 2010. Account updates, new registrations or surveys must be received by Cole-Parmer on or before 11:59 p.m. Central Standard Time on the last day of a particular month to qualify for that month’s drawing.

    Terms and Conditions

  1. No alternative prize, cash or other substitution is permitted except by Cole-Parmer in the event of prize unavailability.
  2. Contest is subject to all applicable rules and laws, and is void where prohibited by law or employer.
  3. From 01/1/2010 thru 03/31/2010. One winner will be chosen each month at random and notified by e-mail. If we are unable to contact you by e-mail within two weeks, your entry will be forfeited and another winner will be chosen.
  4. Participants must be at least 18 years old to win.
  5. Customers and employees of customers which have outstanding overdue balances owed Cole-Parmer Instrument Company or Cole-Parmer Canada are ineligible to participate.
  6. By accepting a prize, the winner explicitly grants his/her permission for Cole-Parmer to post his/her name and company name on ColeParmer.com
  7. No purchase necessary to win.
  8. Employees of Cole-Parmer Instrument Company and its parent, subsidiary and affiliated companies are ineligible to participate.
  9. Contest valid through 03/31/10.

Amazon is not a participant or sponsor of this promotion.

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Clearance Store – 75% off of everything!

Posted by Cole-Parmer on January 7, 2010

Check out the Cole-Parmer Clearance Store.  We’re selling everything at 75% off!
Here are some of our featured products:
Kevlar Gloves – $2.63 a pair
Ideal for handling broken glass or sharp metal parts
Perfect Fit Tuff-Coat II™ Gloves; size, medium 
Giant Diswasher-safe Clear Food Bins  – $18.90 each
Use the colander/drain tray to separate excess moisture from your food to keep it extra fresh.
Carb-x® Food boxes 
Carbon Monoxide Monitor - $182.50
Highly visible flashing red and loud 85dB audible alarms quickly warn you when gas concentration reaches dangerous levels.
Canary II Single Gas Monitor, Carbon Monoxide
 
View our other items in the Clearance Store at this location:  http://www.coleparmer.com/catalog/clearancestore.asp?promo=P9_9/28/2009&referred_id=5618

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